DEPOSITION TEMPERATURE INFLUENCE ON THE MECHANICAL PROPERTIES OF NIOBIUM NITRIDE THIN FILMS
Abstract
Niobium nitride is used in different applications due to its mechanical, tribological, electrical, and optical properties. This paper is a study concerning the influence of the deposition temperature on the mechanical characteristics of niobium nitride thin films at nanoscale. The films were deposited on silicon substrates by direct current magnetron sputtering at different temperatures. The deposition was done at room temperature, at 200 and 400 °C respectively. Atomic force microscopy investigations were performed to determine the mechanical properties of the niobium nitride films. The results pointed out that both the nanohardness and modulus of elasticity are decreasing with the increase in temperature up to 200 °C after which they are increasing when the temperature is increased up to 400 °C.
Key words: niobium nitride, magnetron sputtering, nanoindentation, nanohardness, modulus of elasticity.
Full Text:
PDFReferences
Du, X. et al., Microstructure and optical characterization of magnetron sputtered NbN thin films, Chinese Journal of Aeronautics, vol. 20, pp. 140-144, 2007.
Cui, X. et al., Effects of heat-treatment on mechanical properties and corrosion resistance of NbN films, Physics Procedia, vol. 50, pp. 433-437, 2013.
Singh, K. et al., Adhesion and wear studies of magnetron sputtered NbN films, Tribology International, vol. 50, pp. 16–25, 2012.
Farha, A. et al., The effect of heat treatment on structural and electronic properties of niobium nitride prepared by a thermal diffusion method, Surface & Coatings Technology, vol. 309, pp. 54–58, 2017.
Stanimirović, Z., Stanimirović, I., Mechanical properties of MEMS materials, Micro Electronic and Mechanical Systems, book edited by: Kenichi Takahata, ISBN 978-953-307-027-8, pp. 572, December 2009, INTECH, Croatia.
Lei Yu et al., Fabrication of niobium titanium nitride thin films with high superconducting transition temperatures and short penetration lengths, IEEE Transactions on Applied Superconductivity, vol. 15, pp. 44-48, 2005.
Huang, C.-L. et al., Characteristics of reactively sputtered niobium nitride thin films as diffusion barriers for Cu metallization, Electronic Materials Letters vol. 9, pp. 593-597, 2013.
Ziegler, M. et al., Superconducting niobium nitride thin films deposited by metal organic plasma-enhanced atomic layer deposition, Superconductor Science and Technology, vol. 26, pp. 025008-5, 2013.
Ufuktepe, Y. et al., Superconducting niobium nitride thin films by reactive pulsed laser deposition, Thin Solid Films, vol. 545, pp. 601-607, 2013.
Mercier, F. et al., Niobium nitride thin films deposited by high temperature chemical vapor deposition, Surface and Coatings Technology, vol. 260, pp. 126-132, 2014.
Refbacks
- There are currently no refbacks.